Astm e562, standard test method for determining volume fraction by systematic manual point count. Image analyzer is a device capable of measuring ferrite content measurement from specimens microstructure directly. An astm e562 industry round robin, astm a923 applicability study, astm a923 industry round robin, and an astm a923 study of the effectiveness of existing foundry solution annealing proceduresmore in the astm e562 study, 5 samples were extracted from various cast austenitic and dss in order to have varying amounts of ferrite. This handy equipment provides rapid and accurate data by using highly mobile digital technology.
Electron beam welding of duplex stainless steel with regulated electron beam welding of duplex stainless steel with regulated heat input pdf download available pin. The development of qualification standards for cast duplex. Volume fraction of ferrite was measured using manual point count per astm e562. Astm e56219 standard test method for determining volume fraction by systematic manual point count. Astm e 562 dss confidence interval accuracy and precision. E562 11 standard test method for determining volume fraction by systematic manual point count attached files a26215 standard practices for detecting susceptibility to intergranular attack in austenitic st. A800a800m standard practice for steel casting, austenitic alloy, estimating ferrite content thereof. Astm e562 02 standard test method for determining volume. Astm e562 19 standard test method for determining volume fraction by systematic manual point count. A comprehensive list of citations to this standard are listed here. Ferrite content measurement is used to measure the ferrite. Intergranular corrosion tests igc two test methods namely a modified astm a262 and a modified double loop electrochemical potentiokinetic.
Ferrite count evaluation of an inservice cru reactor. I am trying to do a % austeniteferrite count on a weld crossection of 2205. Techniques and standards for measuring ferrite in austenitic. Duplex stainless steel, welding, ferrite content, point count, astm e562, image analysis. Characterization of the weld regions within duplex stainless steels using magnetic force microscopy. Ten fields per sample were analyzed at 500x magnification. The astm grainsize scale was established using the imperial system of units, but no difficulty is introduced by metric measurements. Astm a800 defines ferrite as the ferromagnetic, bodycentered cubic, microstructural constituent of variable chemical composition in ironchromiumnickel alloys. Download free astm e562 11 techstreet separately the documents listed below are referenced within the subject standard but are not provided as part of the standard.
When working with metals, metallurgical testing helps to detect material flaws, determine microstructural features, evaluate heat treatments and assure compliance to required specifications. Duplex stainless steel 97, 5th world conference, 2123 october 1997, maastricht, the netherlands, 1997. B499 test method for measurement of coating thicknesses by the magnetic method. Mark henning grain metallographic phase analysis, grain. The average area of the particles can be calculated by dividing the volume fraction, vv, by na. Astme562 complete document history standard test method for determining volume fraction by systematic manual point count. All services are performed at our onestop facility near philadelphia, pa usa. A941 terminology relating to steel, stainless steel, related alloys, and ferroalloys. We test and analyze all types of ferrous and nonferrous metals and alloys, including precious metals and powdered metals. Astm e56211 standard test method for determining volume fraction by systematic manual point count. Microscopic examination of metals laboratory testing inc.
Jun 28, 2019 ferrite testing is a technique used to measure the delta ferrite content in austenitic stainless steel and duplex stainless steel. Ferrite count evaluation of an inservice cru reactor center. Hence, the number of particles per unit area, n a, is 0. Final report, volume 2, the development of qualification. Determination of volume fraction astm e562 ferrite content. Optimal etching sequence for austenite to ferrite ratio. The phase balance is commonly determined as a part of the duplex stainless steel dss welding procedure qualification. In this work, the aim was to find a reliable, but still fast method to measure the ferrite content of dss welds. Study on ferrite measurement methods for duplex stainless. The produced micrographs were then analyzed in consonance with the requirements of astm e562 05 using microstructure characterizer software, mic 2. Astm e562 standard test method for determining volume. Astm e562, standard test method for determining volume. Astm e2318 astm a37017a hardness brinell hardness hb 5125 hb 5250 astm e1018 metallurgical tests ferrite manual point count astm e56211 ferrite automatic image analysis astm e1245032016 corrosion tests pitting corrosion resistance astm g48112015 practice a astm a92314 practice c end. The test uses a portable feritscope machine from fischer.
Ferrite content in the heat affected zone of duplex stainless. The results have suggested a necessity of establishment of standardized testing variables to be used for ferrite measurement with manual point count according to astm e562. Stainless, instrument calibration, for estimating ferrite content. Metallurgical testing, metallography laboratory testing inc.
E56211 standard test method for determining volume fraction by systematic manual point count attached files a26215 standard practices for detecting susceptibility to intergranular attack in austenitic st. Mvmtc offers a variety of metallurgical analysis procedures such as micro. The results obtained showed that the ferrite count for the scallops and center pipe of reactor. Ferrite testing mechanical testing testing services. The volume fraction vf of ferrite was determined from the astm e562 point count method. Astme562 standard test method for determining volume. Ferrite quantification methodologies for duplex stainless steel.
Astm e562 19 standard test method for determining volume. Counting ferriteaustenite % in duplex microstructure. For this measurement method, there are several testing variables and it seems. Superseded see active link, below download standard pdf more info. These services are also called metallography evaluation, metallographic examination and metallurgical analysis. Ferrite measurement in austenitic and duplex stainless steel. E562 test method for determining volume fraction by systematic manual point count. Astm e562 11 standard test method for determining volume fraction by systematic manual point count active standard astm e562 developed by subcommittee. Automatic ferrite content measurement based on image. The measured austenite ratios in case of the astm e562 manual point count method ar astm for ldx 2101 were 27. Influence of the shielding gas composition on the passive. Ferrite testing is a technique used to measure the delta ferrite content in austenitic stainless steel and duplex stainless steel. Astm standard e56202, using an image analysis routine with leica qmetals software, connected to a leica dmlm microscope. Sep 30, 2005 volume fraction of ferrite was measured using manual point count per astm e562.
E562111 item s proposed revisions of this standard. Volume 2 deals with the development of qualification standards for cast duplex stainless steel a8904a which is equivalent to wrought 2205. Methods for the measurement of ferrite content in multipass. Astm international standard references for astm e562 19. Standard test method for determining volume fraction by systematic manual point count 1. Point counting was done on a minimum of two photomicrographs of each stan dard using a grid of 1032 points each time. Astm a799 a799m 102020 standard practice for steel. An astm designation number identifies a unique version of an astm standard. When duplex stainless steel dss is applied to welded components, ferrite measurement with manual point count according to astm 1 e562 is often used during welding procedure qualification as heat affected zone haz of the weld tends to have high ferrite content. The ferrite content of the welding procedures were measured by the astm e562 point count method production welds were tested using a ferritscope however the specification gave the same acceptance value for ferrite content and ferrite number. Ferrite count 316ss astm e562 metengr materials 9 aug 07 07. Counting ferriteaustenite % in duplex microstructure steel. Results indicate that astm e562 is applicable to dss and the results have excellent labtolab reproducibility. Astm e56208 standard test method for determining volume fraction by systematic manual point count superseded see active link, below.
Sometimes, phase analysis tends to be a boring job. I am trying to do a % austenite ferrite count on a weld crossection of 2205. These parameters can be related to the astm grain size number, g. Apr 10, 2019 the phase balance is commonly determined as a part of the duplex stainless steel dss welding procedure qualification. A799a799m standard practice for steel castings, stainless, instrument calibration, for estimating ferrite content.
Ferrite count 316ss astm e562 astm testing materials. Astm e56208, standard test method for determining volume fraction by systematic manual point count 4 bonnefois, b soulignac, p statistical system of prediction for duplex and superduplex weld properties, in. Astm e562 05 standard test method for determining volume. When used in combination with energy dispersive xray spectroscopy eds, the microstructure analysis can identify inclusion type and corrodents on the fracture face. In the astm e562 study, 5 samples were extracted from various cast austenitic and dss in order to have varying amounts of ferrite.
Astm e562 11 standard test method for determining volume fraction by systematic manual point count. For this measurement method, there are several testing variables and it seems that standard testing variables are not. This may be formed upon solidification from the molten metal delta ferrite or by transformation from austenite or sigma phase on cooling in the solid state alpha ferrite. Ferrite quantification methodologies for duplex stainless. The delta ferrite content is measured to better understand an austenitic or duplex stainless steels susceptibility to corrosion, susceptibility to solidification cracking and other types of material failure. Ferrite measurement in austenitic and duplex stainless. Ferrite count 316ss astm e562 astm testing materials code dont count out undergraduate research. Astm e562 05 standard test method for determining volume fraction by systematic manual point count. The produced micrographs were then analyzed in consonance with the requirements of astm e56205 using microstructure characterizer software, mic 2. Astme562 standard test method for determining volume fraction by systematic manual point count astme562 2019 edition current show complete document history how to order. Metal testing and alloy testing are specialties of laboratory testing inc.
On the other hand, scanning electron microscopy is used to determine abnormalities such as inclusions, segregation, and surface layers, as well as fracture features. A565 a565m standard specification for martensitic stainless steel bars for hightemperature service. American society for testing materials astm e562 7 standard describes the detailed procedure for the measurement of volume fraction of ferrite. Ferrite count 316ss astm e562 astm testing materials code. Metallurgical testing typically uses microscopy to provide important information about the structure and properties of metal and alloy samples. An astm e562 industry round robin, astm a923 applicability study, astm a923 industry round robin, and an astm a923 study of the effectiveness of existing foundry solution annealing proceduresmore. The accuracy of desired results is strictly dependent on the. Astm e56211 standard test method for determining volume. Ferrite measurements the ferrite content of each stan dard was determined by point count ing, the severn gage, the magne gage, and the ferrite meter. In order to quantify ferrite content, three techniques, xrd, ferritoscope and optical metallography, were applied to a duplex stainless steel uns s31803 solutiontreated for 30 min at 1,000, 1,100 and 1,200 c, and then compared to equilibrium of phases predicted by thermocalc simulation. Ferrite content measurement, also known as a ferritescope test at nusatek, is a nondestructive test and normally performed on site. I have the standard, but have never used it before. Metal testing, alloy testing laboratory testing inc.
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